3d_imaging

Purdue University 3D X-ray Microscope facility

About the Facility & Services

The Purdue University 3D X-Ray Microscope Shared User Facility was launched in December 2017. The acquisition of the Zeiss Xradia 510 Versa 3D X-ray Microscope was supported by the EVPRP Major Multi-User Equipment Program 2017 at Purdue University. The equipment is available to all researchers on campus and external to Purdue University (Academic and Non-academic), and we accept research collaborations in all areas. 

The Facility is managed by Dr. Laura Pyrak-Nolte with the assistance of Super Users who implement 3D imaging tomographic recipes and perform all scanning and analysis of the resulting 3D imaging data. To ensure that we provide the best data possible, we generally utilize in-house fabricated sample holders which improve sample positioning and data-registration abilities especially for situations where time-dependent scanning is needed.

We recommend that any researcher interested in 3D X-Ray imaging to connect with us for a consultation so you can decide if the Zeiss Xradia 510 Versa 3D X-Ray Microscope is the best for your research needs. 

Click here for information on available equipment and sample requirements.

 

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Dr. Laura Pyrak-Nolte

3D XRM Facility Manager

Distinguished Professor 

Department: Physics & Astronomy

Office: PHYS 164

Phone: (765) 494-3027

Email: ljpn@purdue.edu

Website: Rock Physics Group

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Chven Mitchell

Super User

PhD. Student - Rock Physics Group

Department: EAPS

Email: mitch240@purdue.edu

 

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Liyang Jiang

Super User

PhD. Student - Rock Physics Group

Department: Physics

Email: jiang352@purdue.edu 

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Ben Denos

Super User for CMSC

Postdoctoral Researcher 

Department: Composites Manufacturing & Simulation Center

Email: denos@purdue.edu

Website: CMSC Group

Scan Provided (per scan hour)
A full-service scan facilitated from start to finish by staff within the recharge center. The analysis service includes 3D reconstruction and visualization. For additional analysis, such as segmentation, porosity analysis, etc. please see the Analysis rate. 
 
Self Scan (per set-up/scan hour)
Service is for Purdue University faculty, staff, and students that have been trained by recharge center staff to effectively, efficiently, and safely use the instrumentation. To utilize this service, a recharge center staff member will train the individual on use of the instrumentation for their first three scans (see training description). The user also has to complete and sign a liability form. Prior to a scan appointment, a completed account information form should be submitted to Prof. Pyrak-Nolte (ljpn@purdue.edu).
 
Training or analysis (per hour) 
Services are (a) charged hourly during the required training for self-scan usage of the 3D XRM Versa 510 System or (b) charged hourly for additional analysis provided by the staff.
  • The trainee must complete and sign both (i) the liability form and (ii) the account information form prior to the initiation of training. The hourly training rate covers set-up and initiation of the scan and post-scan finalization and validation of the scan. On average, each of the three training session will last approximately 3 hours (at the Training rate) plus the scan time. During training scans, the cost for X-ray scanning time will be billed at the Self Scan hourly rate. The training and scan time may vary based on the complexity of the scan among other factors. The center staff retains the right to require additional training if the user is deemed not fully competent after 3 training sessions. 
 
  • The analysis rate applies to requests for additional analysis of the scans (e.g. segmentation, porosity analysis, etc) performed by the center staff.
 
Exploratory Analysis (per set-up hour + analysis time)
Services are performed by the staff and recommended for situations where a researcher have never performed micro-CT on a sample, does not know the feature location and also if the scan parameters are unknown for a particular sample (e.g. number of projections and/or different exposure times) to determine if the desired information can be obtained for their specific material and structure. These exploratory analyses require additional effort by the recharge center staff to mount the sample, set-up and explore scan parameters as directed for the specific material/structural feature, and analysis for visualization. After the exploratory analysis, if a customer decides to proceed with a full 3D scan, the full scan would then be billed at the Scan Provided (per scan hour) rate.
We have utilized the 3D X-Ray Microscope to obtain 3D and 2D imaging datasets for many applications, and welcome new samples to scan and expand our abilities. 
Please Explore the Publications which include data that display the imaging capabilities of this facility. Some of the successful Applications performed at our facility:
  • Image the pore spaces within a mass of fat crystals
  • Image the defects accumulated within stainless steel after cyclic loading
  • 2D imaging of time-dependent crack formation within geo-architected rocks
  • 3D imaging of crack formation after 3-point bending and other deformation
  • 3D measurement of precipitate build up after flow experiments
  • 3D imaging of 3D printed steel to evaluate deposits within pore spaces
  • 2D & 3D imaging of specimen during in-situ tensile/compression testing using a Debens Testing Stage (Ask us about this equipment)
  • 3D & 2D measurements of fluid movement in materials and microfluidic devices
  • 3D measurement of induced cracks, and drying-induced damage to geo-architected rocks 
  • Fiber thickness and density measurements from 3D imaging of the fabric of different types of fibers (ceramic, glass, wood, steel, etc.) in different configurations (packed, pressed, woven, mats) 
  • 3D imaging of fractured surfaces and roughness in 3D printed rock analogs
  • 3D analysis of 3D‐printed hardened cement paste (hcp) elements, to evaluate the heterogeneous interfaces fabricated with novel architectures
  • Detection and analysis of fractures in trabecular bone 
  • Evaluation of aggregate distribution and porosity of concrete and cement mortar cores
  • 3D measurement of porosity in Sandstone and shale cores
  • 3D carbon fiber orientation, foliations, and inter-connected network properties 
  • 3D imaging of cement boreholes
  • Scout, Scan, and Zoom for samples where large FOV and high-resolution image datasets are needed
  • Imaging grain displacement and particle crushing 
  • Compacted soil
  • Pore structure of Pharmaceuticals

 

Departments and Institutions that have utilized our facility.
Internal (On Campus or Purdue University Affiliated)
Agricultural Sciences
Agronomy
Bio-Medical Engineering
Civil Engineering
Composites Manufacturing and Simulation Center at Purdue University
Earth, Atmospheric, and Planetary Sciences
Enhanced Oil Recovery Lab at Purdue University
Industrial Engineering
Mechanical Engineering
Materials Science Engineering
Physics and Astronomy

External (Non-Purdue: Academic & Non-Academic)
University of Alabama - Mechanics of Materials under Extreme Environments Group
Ohio State University - Food Science and Technology
Princeton University
Sandia National Laboratory - Geomechanics

 

All publications that contain data obtained from imaging at the Facility should acknowledge the 3D XRM Facility's contribution as follows:
  • If scanning and/ image analysis and segmentation were performed by any of the 3D XRM personnel please acknowledge as follows:
Acknowledgment:  We acknowledge Chven Mitchell who assisted/acquired the images of XXX for this paper on a Zeiss Xradia 510 Versa 3D X-ray Microscope that was supported by the EVPRP Major Multi-User Equipment Program 2017 at Purdue University.
  • If all scanning and image analysis was self-run, please acknowledge as follows:
Acknowledgment:  We acknowledge the 3D X-Ray Microscope Facility in the Department of Physics for the images of XXX shown in this paper, which were acquired on a Zeiss Xradia 510 Versa 3D X-ray Microscope that was supported by the EVPRP Major Multi-User Equipment Program 2017 at Purdue University.

We do accept scanning request from external clients (researchers at institutions external to Purdue University both academic and non-academic). At current we are not allowing external users to utilize the 3D X-Ray Microscope for self-scanning.

When requesting services an external user can only make a requested for Exploratory Analysis, Exploratory Scans, or Scan provided (See Services for more information). Please feel free to contact us for more information or for a 3D X-Ray Imaging consultation.


Scanning Rates for External Entities

Scan Provided (per scan hour) $52.00
Exploratory Analysis (per set-up and/ scan hour) $63.00


Shipping Samples:
Approval MUST be obtained before shipping a sample to the 3D XRM Facility. We will not accept any samples without prior notification. Please contact us to discuss your 3D imaging needs and shipping.

Shipping Address:
c/o Dr. Laura Pyrak-Nolte
Purdue University
Department of Physics & Astronomy
525 Northwestern Avenue
West Lafayette
IN, 47907
We welcome visitors to the Purdue's 3D XRM Facility. Please feel free to contact us to schedule an appointment and tour of the lab. 


Location:

Purdue University
Department of Physics & Astronomy
Room G48
525 Northwestern Avenue
West Lafayette
IN, 47907

Nearest paid parking garage:
Grant Street Parking Garage
120 Grant St, West Lafayette, IN 47906

Note:
2-hour parking is also available on residential streets near the Department of Physics & Astronomy


Shipping Samples:

Approval MUST be obtained before shipping a sample to the 3D XRM Facility. We will not accept any samples without prior notification. Please connect with us to discuss your 3D imaging needs and shipping.

Shipping Address:
c/o Dr. Laura Pyrak-Nolte
Purdue University
Department of Physics & Astronomy
525 Northwestern Avenue
West Lafayette
IN, 47907


Lodging within a mile of Purdue University:

Purdue Memorial Union Club Hotel (Currently Under Renovation)





Interested in 3D X-Ray Imaging. Explore our Publications before you go.